（一）、金属化合物的测定    辽宁聚实环保

SHUITIZHONGDEJINSHUYUANSUYOUXIESHIRENTIJIANKANGBIXUDECHANGLIANGYUANSUHEWEILIANGYUANSU，YOUXIESHIYOUHAIYURENTIJIANKANGDE，RUGONG、GE、GE、QIAN、SHEN、TONG、XIN、NIE、BEI、FANDENG。SHOU“SANFEI”WURANDEDIMIANSHUIHEGONGYEWUSHUIZHONGYOUHAIJINSHUHUAHEWUDEHANLIANGWANGWANGMINGXIANZENGJIA。YOUHAIWUZHIQINRURENTIDEJITIHOU，JIANGHUISHIMOUXIEMEISHIQUHUOXINGERSHIRENTICHUXIANBUTONGCHENGDUDEZHONGDUZHENGZHUANG。CEDINGSHUITIZHONGJINSHUYUANSUGUANGFANCAIYONGDEFANGFAYOUFENGUANGGUANGDUFA、YUANZIXISHOUFENGUANGGUANGDUFA、RONGLIANGFA。

1、GONGDECEDING：GONGJIQIHUAHEWUSHUYUJUDUWUZHI，WUJIYANZHONGYILVHUAGONGDUXINGZUIDA，YOUJIGONGYIJIAJIGONG、YIJIGONGDUXINGZUIDA。GONGSHIWEIYIYIGECHANGWENXIACHENGYETAIDEJINSHU，YIHUIFAJINRURENTIHUXIDAO，YIKEWEIPIFUXISHOU，ZAOCHENGGONGZHONGDU。SHUITIZHONGDEWEILIANGGONGKEJINGSHIWULIANCHENGBAIWANBEIDEFUJI，YINFA“SHUIYUBING”。TIANRANSHUIZHONGHANGONGJISHAO，YIBANBUCHAOGUO0.1μg/L。WOGUOYINYONGSHUIBIAOZHUNXIANZHIWEI0.001mg/L。GONGDEZUIDIJIANCHUNONGDUWEI2μg/L，CEDINGSHANGXIANWEI40μg/L。FANGFASHIYONGYUGONGYEWUSHUIHESHOUGONGWURANDEDIMIANSHUIDEJIANCE。

CEDINGFANGFA：LENGYUANZIXISHOUFA、SHUANGLIUZONGFENGUANGGUANGDUFA

2、GEDECEDING：GEZAINONGDUHENDIDEQINGKUANGXIADOUJUYOUHENQIANGDEDUXING，KEZAIRENTIDEGAN、SHENDENGZUZHIZHONGXUJI，ZAOCHENGGEZANGQIZUZHIDESUNHUAI，YOUYIDUISHENZANGSUNHAIZUIWEIMINGXIAN。HAIKEYIDAOZHIGUZHISHUSONGHERUANHUA。GEZAITURANGHEYANSHIZHONGDEZIRANCUNZAI，TONGCHANGQINGKUANGXIAYUXINJIQIHUAHEWUGONGCUN。JUEDADUOSHUDANSHUIDEHANGELIANGDIYU1μg/L，HAISHUIZHONGGEDEPINGJUNNONGDUWEI0.15μg/L。GEDEZHUYAOWURANYUANSHIDIANDU、CAIKUANG、YELIAN、RANLIAO、DIANCHIHEHUAXUEGONGYEDENGPAIFANGDEWUSHUI。

CEDINGFANGFA：（CEDINGGE、TONG、QIAN、XINDENGYUANSUSHI）ZHIJIEHUOYANYUANZIXISHOUFENGUANGGUANGDUFA（SHIYONGYUWUSHUIHESHOUWURANDESHUI）CUIQUHUOLIZIJIAOHUANFAFUJIFAAS（SHIYONGYUQINGJIESHUI）SHIMOLUAAS（SHIYONGYUQINGJIESHUI，QICEDINGLINGMINDUGAOYUQIANLIANGZHONGFANGFA，DANJITIGANRAOJIAOHUOYANYUANZIHUAFAYANZHONG）

A、ZHIJIEXIRUFAASCEDINGGE（TONG、QIAN、XIN） QINGJIESHUIYANGKEBUJINGYUCHULIZHIJIECEDING；WURANDEDIMIANSHUIHEWUSHUIXUYONGXIAOSUANHUOXIAOSUAN-GAOLVSUANXIAOJIE，BINGJINXINGGUOLV、DINGRONG。

DINGLIANGFENXIFANGFA：BIAOZHUNQUXIANFA、BIAOZHUNJIARUFA  CEDINGTIAOJIANHEFANGFASHIYONGNONGDUFANWEILIEYUBIAO2-9。

B、SHUANGLIUZONGFENGUANGGUANGDUFA

YUANLI：FANGFAJIYUZAIQIANGJIANXINGJIEZHIZHONG，GELIZIYUSHUANGLIUZONGSHENGCHENGHONGSEAOHEWU，YONGSANLVJIAWANCUIQUFENLIHOU，YU518nmCHUCEQIXIGUANGDU，YUBIAOZHUNRONGYEBIJIAODINGLIANG。GANRAOQINGKUANG：SHUIYANGZHONGHANQIAN20mg/L、XIN30mg/L、TONG40mg/L、MENGHETIE4mg/L，BUGANRAOCEDING，MEILIZINONGDUDA20mg/LSHI，XUDUOJIAJIUSHISUANJIANAYANBI。BENFANGFASHIYONGYUSHOUGEWURANDETIANRANSHUIHEWUSHUIZHONGGEDECEDING，CEDINGQIANYINGDUISHUIYANGJINXINGXIAOJIECHULI。

3、QIANDECEDING         QIANSHIKEZAIRENTIHEDONGZHIWUZUZHIZHONGXUJIDEYOUDUJINSHU，QIZHUYAODUXINGXIAOYINGSHIDAOZHIPINXUE、SHENJINGJINENGSHIDIAOHESHENSUNSHANGDENG。QIANDUISHUISHENGSHENGWUDEANQUANNONGDUWEI0.16mg/L。QIANDEZHUYAOWURANYUANSHIXUDIANCHI、YELIAN、WUJIN、JIXIE、TULIAOHEDIANDUGONGYEDENGBUMENDEPAIFANGWUSHUI。

CEDINGFANGFA：CEDINGSHUITIZHONGQIANDEFANGFAYUCEDINGGEDEFANGFAXIANGTONG。GUANGFANCAIYONGYUANZIXISHOUFENGUANGGUANGDUFAHESHUANGLIUZONGFENGUANGGUANGDUFA，YEKEYIYONGYANGJIRONGCHUFUANFAHESHIBOJIPUFA。          SHUANGLIUZONGFENGUANGGUANGDUFAJIYUZAIpH8.5—9.5DEANXINGNINGMENGSUANYAN-QINGHUAWUDEHAIYUANJIEZHIZHONG，QIANYUSHUANGLIUZONGFANYINGSHENGCHENGHONGSEAOHEWU，YONGSANLVJIAWAN（HUOSILVHUATAN）CUIQUHOUYU510nmBOZHANGCHUBISECEDING。          CEDINGSHI，YAOTEBIEZHUYIQIMIN、SHIJIJIQULIZISHUISHIFOUHANHENLIANGQIAN，ZHEISHINENGFOUHUODEZHUNQUEJIEGUODEGUANJIAN。Bi3+、Sn2+DENGGANRAOCEDING，KEYUXIANZAIpH2—3SHIYONGSHUANGLIUZONGSANLVJIAWANRONGCUIQUFENLI。WEIFANGZHISHUANGLIUZONGBEIYIXIEYANGHUAWUZHIRUFe3+DENGYANGHUA，ZAIANXINGJIEZHIZHONGJIARULEYANSUANQIANGAN。

4、TONGDECEDING        TONGSHIRENTISUOBIXUDEWEILIANGYUANSU，QUETONGHUIFASHENGPINXUE、FUXIEDENGBINGZHENG，DANGUOLIANGSHERUTONGYIHUICHANSHENGWEIHAI。TONGDUISHUISHENGSHENGWUDEWEIHAIJIAODA，YOURENRENWEITONGDUIYULEIDEDUXINGNONGDUSHIYU0.002mg/L，DANYIBANRENWEISHUITIHANTONG0.01mg/LDUIYULEISHIANQUANDE。TONGDUISHUISHENGSHENGWUDEDUXINGYUQIXINGTAIYOUGUAN，YOULITONGLIZIDEDUXINGBILUOHETAITONGDADEDUO。SHIJIEFANWEINEI，DANSHUIPINGJUNHANTONG3μg/L，HAISHUIPINGJUNHANTONG0.25μg/L。TONGDEZHUYAOWURANYUANSHIDIANDU、YELIAN、WUJINJIAGONG、KUANGSHANKAICAI、SHIYOUHUAGONGHEHUAXUEGONGYEDENGBUMENPAIFANGDEWUSHUI。

CEDINGFANGFA：ERYIANJIERLIUDAIJIASUANNACUIQUFENGUANGGUANGDUFA、XINYATONGLINGCUIQUFENGUANGGUANGDUFA

5、GEDECEDING     GEHUAHEWUDECHANGJIANJIATAIYOUCr(Ⅲ)HECr(Ⅵ) ，SHOUSHUIWEN、pHZHI、YANGHUAHAIYUANWUZHI、YOUJIWUDENGYINSUDEYINGXIANG，ERZHEZHIJIANKEYIHUXIANGZHUANHUA。GEDEDUXINGYUQICUNZAIJIATAIYOUGUAN。GEDEGONGYEWURANYUANZHUYAOLAIZIGEKUANGSHIJIAGONG、JINSHUBIAOMIANCHULI、PIGEROUZHI、YINRAN。ZHAOXIANGCAILIAODENGXINGYEDEWUSHUI。GESHISHUIZHIWURANKONGZHIDEYIXIANGZHONGYAOZHIBIAO。

（1）LIUJIAGEDECEDING ZAISUANXINGJIEZHIZHONG，LIUJIAGEYUERBENTANXIANERJING（DPC）FANYING，SHENGCHENGZIHONGSELUOHEWU，YU540nmBOZHANGCHUJINXINGBISECEDING。          BENFANGFAZUIDIJIANCHUNONGDUWEI0.004mg/L，SHIYONG10mmBISEMIN，CEDINGSHANGXIANWEI1mg/L。QICEDINGYAODIANRUXIA： DUIYUQINGJIESHUIYANGKEZHIJIECEDING； DUIYUSEDUBUDADESHUIYANG，KEYONGYIBINGTONGDAITIXIANSEJIDEKONGBAISHUIYANG ZUOCANBICEDING； DUIYUHUNZHUO、SEDUJIAOSHENDESHUIYANG，YIQINGYANGHUAXINZUOGONGCHENDIANJI，DIAOJIERONGYEpHZHI8—9，CISHICr3+、Fe3+、Cu2+JUNXINGCHENGCHENDIANBEIGUOLVCHUQU；CUNZAIYALIUSUANYAN、ERJIATIEDENGHAIYUANXINGWUZHIHECILVSUANYANDENGYANGHUAXINGWUZHISHI，YEYINGCAIQUXIANGYINGXIAOCHUGANRAOCUOSHI。

（2）ZONGGEDECEDING ZAISUANXINGRONGYEZHONG，SHOUXIAN，JIANGSHUIYANGZHONGDESANJIAGEYONGGAOMENGSUANJIAYANGHUACHENGLIUJIAGE，GUOLIANGDEGAOMENGSUANJIAYONGYAXIAOSUANNAFENJIE，GUOLIANGDEYAXIAOSUANNAYONGNIAOSUFENJIE；RANHOU，JIARUERBENTANXIANJINGXIANSE，YU540nmCHUJINXINGFENGUANGGUANGDUCEDING。QIZUIDIJIANCHUNONGDUTONGLIUJIAGE。QINGJIEDIMIANSHUIKEZHIJIEYONGGAOMENGSUANJIAYANGHUAHOUCEDING；SHUIYANGZHONGHANDALIANGYOUJIWUSHI，YONGXIAOSUAN－LIUSUANXIAOJIE。LIUSUANYATIEANDIDINGFA：           BENFASHIYONGYUZONGGENONGDUDAYUImg／LDEWUSHUI。QIYUANLIWEIZAISUANXINGJIEZHIZHONG，YIYINYANZUOCUIHUAJI，YONGGUOLIUSUANANJIANGSANJIAGEYANGHUACHENGLIUJIAGE。JIASHAOLIANGLVHUANABINGZHUFEI，CHUQUGUOLIANGDEGUOLIUSUANANHEFANYINGZHONGCHANSHENGDELVQI。YIBENJIDAILINANJIBENJIASUANZUOZHISHIJI，YONGLIUSUANYATIEANBIAOZHUNRONGYEDIDING，ZHIRONGYECHENGLIANGLVSE。